tio2 e171

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The raw material used in this method is FeSO4. In order to maintain the Fe3 + concentration in the reaction medium in a specific range, reducing agent iron sheet is added in the reaction process. Iron yellow crystal seed was added and air was introduced to synthesize iron yellow under certain pH conditions. The method mainly includes two steps: (1) firstly, FeSO4 · 7H2O is used as raw material, NaOH or NH3 · H2O is used as precipitant or pH regulator, and air is used as oxidant to prepare crystal seed; (2) Iron yellow is produced by two-step oxidation with crystal seed, FeSO4, iron sheet and air.

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In recent years, instrumental techniques have gained prominence for their speed and precision. Ion chromatography, for instance, separates and quantifies ions based on their affinity to a resin within a chromatographic column. The sulfate ions are eluted and detected, typically by conductivity or UV detection after reaction with a reagent that enhances their detectability. The area under the peak in the chromatograph is proportional to the concentration of sulfate, which can then be translated to TiO2 content through appropriate calculations.

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